Crystallographic data collection statistics
Wavelength, Å | 0.9795 |
| Beamline | ID23-1* |
| Crystal to detector distance, mm | 275.91 |
| Space group | P212121 |
| Unit cell parameters, Å | |
| A | 41.90 |
| B | 62.80 |
| C | 122.80 |
| Resolution range, Å | 19.88-2.32 |
| R | 8.7 |
| I/Sigma (I) | 14.08 (3.13)† |
| Completeness, % | 86.9 (56.7)† |
| Redundancy | 6.024 (3.7)† |
| Final model statistics (refinement) | |
| Resolution limits, Å | 19.88-2.32 (2.375-2.315)† |
| No. reflections used for refinement | 12 211 |
| No. reflections in the test set | 645 |
| R, % | 21.35 |
| Rfree, % | 25.55 |
| RMSD bonds/angles, Å/° | 0.012/1.463 |
| No. residues in Ramanchandran | 244 |
| Residues in most favored regions, % | 87.7 |
| Residues in additional allowed regions, % | 12.3 |
| Residues in generously allowed regions, % | 0 |
| No. protein atoms | 1 537 |
| No. water atoms | 28 |
| Average B factor, Å2 | 58.354 |
| B factor from Wilson plot, Å2 | 52.0 |
Wavelength, Å | 0.9795 |
| Beamline | ID23-1* |
| Crystal to detector distance, mm | 275.91 |
| Space group | P212121 |
| Unit cell parameters, Å | |
| A | 41.90 |
| B | 62.80 |
| C | 122.80 |
| Resolution range, Å | 19.88-2.32 |
| R | 8.7 |
| I/Sigma (I) | 14.08 (3.13)† |
| Completeness, % | 86.9 (56.7)† |
| Redundancy | 6.024 (3.7)† |
| Final model statistics (refinement) | |
| Resolution limits, Å | 19.88-2.32 (2.375-2.315)† |
| No. reflections used for refinement | 12 211 |
| No. reflections in the test set | 645 |
| R, % | 21.35 |
| Rfree, % | 25.55 |
| RMSD bonds/angles, Å/° | 0.012/1.463 |
| No. residues in Ramanchandran | 244 |
| Residues in most favored regions, % | 87.7 |
| Residues in additional allowed regions, % | 12.3 |
| Residues in generously allowed regions, % | 0 |
| No. protein atoms | 1 537 |
| No. water atoms | 28 |
| Average B factor, Å2 | 58.354 |
| B factor from Wilson plot, Å2 | 52.0 |